ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

Base Information

Chemical Name:ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate
CAS No.:859831-71-3
Molecular Formula:C₃₄H₃₃NO₅
Molecular Weight:535.64
Hs Code.:

Synonyms:ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

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Chemical Property of ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

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Technology Process of ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

There total 4 articles about ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859831-66-6
4-(2-(2-benzyloxycarbazol-9-yl)ethoxy)benzaldehyde

: 13676-06-7
ethyl 2-ethoxy-2-(diethylphosphono)acetate

: 859831-71-3
ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2005.04.018

Reference yield:

: 86-79-3
2-hydroxycarbazole

: 859831-71-3
ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammonium hydrogen sulfate; potassium carbonate / ethyl acetate / Heating

2: sodium hydride / tetrahydrofuran / 0 - 20 °C

3: sodium hydride / tetrahydrofuran / 0 - 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; potassium carbonate; In tetrahydrofuran; ethyl acetate; 3: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.bmc.2005.04.018

Reference yield:

: 52191-15-8
4-(2-bromoethyloxy)benzaldehyde

: 859831-71-3
ethyl 2-ethoxy-3-{4-[2-(2-benzyloxycarbazol-9-yl)ethoxy]phenyl}-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 0 - 20 °C

2: sodium hydride / tetrahydrofuran / 0 - 20 °C

With sodium hydride; In tetrahydrofuran; 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.bmc.2005.04.018