9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

Base Information

Chemical Name:9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester
CAS No.:1186532-36-4
Molecular Formula:C₁₅H₁₈Cl₂N₂O₂
Molecular Weight:329.226
Hs Code.:

Synonyms:9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

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Chemical Property of 9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

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Technology Process of 9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

There total 6 articles about 9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 90152-00-4
9-methyl-3,9-diazabicyclo<3.3.1>nonane

: 72305-24-9
3,4-dichlorophenyl chloroformate

: 1186532-36-4
9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

Guidance literature:: 9-methyl-3,9-diazabicyclo<3.3.1>nonane; 3,4-dichlorophenyl chloroformate; In 1,2-dimethoxyethane; at 20 ℃; for 15h;

With ammonia; In 1,2-dimethoxyethane; water;

Reference yield:

: 182949-96-8
diethyl cis-1-methylpiperidine-2,6-dicarboxylate

: 1186532-36-4
9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: xylene / 205 °C / Reflux; Inert atmosphere

2.1: lithium aluminium tetrahydride / 1,4-dioxane / 18 h / Reflux

2.2: 80 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 100 °C / 45004.5 Torr

4.1: 1,2-dimethoxyethane / 15 h / 20 °C

With lithium aluminium tetrahydride; hydrogen; palladium 10% on activated carbon; In 1,4-dioxane; 1,2-dimethoxyethane; ethanol; xylene;

Reference yield:

: 111-16-0
heptanedioic acid

: 1186532-36-4
9-methyl-3,9-diaza-bicyclo[3.3.1]nonane-3-carboxylic acid 3,4-dichloro-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 40 - 100 °C

1.2: 3 h / UV-irradiation

2.1: tetrahydrofuran / 18 h / Cooling; Inert atmosphere

3.1: xylene / 205 °C / Reflux; Inert atmosphere

4.1: lithium aluminium tetrahydride / 1,4-dioxane / 18 h / Reflux

4.2: 80 °C

5.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h / 100 °C / 45004.5 Torr

6.1: 1,2-dimethoxyethane / 15 h / 20 °C

With lithium aluminium tetrahydride; thionyl chloride; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; ethanol; xylene;