methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Base Information

• Chemical Name: methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside
• CAS No.: 294637-59-5
• Molecular Formula: C₃₇H₄₄O₆Si
• Molecular Weight: 612.838

Synonyms:methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Chemical Property of methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside

There total 4 articles about methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

methanol (67-56-1) + 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-D-glucal (137792-57-5) → methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside (294637-59-5)

Guidance literature:

3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-D-glucal; With DMDO;

methanol; Further stages.;

DOI:10.1021/ja0008665

Reference yield:

(o-biphenyl)P(t-Bu)2 + N-methylaniline (100-61-8) + methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-(4-chlorobenzyl)-β-D-glucopyranoside (294637-51-7) → methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside (294637-59-5)

Guidance literature:

With tin(IV) chloride; sodium t-butanolate; palladium diacetate; In dichloromethane;

Reference yield:

{4-[(2R,3R,4S,5R,6R)-4,5-Bis-benzyloxy-6-(tert-butyl-diphenyl-silanyloxymethyl)-2-methoxy-tetrahydro-pyran-3-yloxymethyl]-phenyl}-methyl-phenyl-amine → methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-glucopyranoside (294637-59-5)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ja0008665

upstream raw materials:

methanol

3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-D-glucal

methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-(4-chlorobenzyl)-β-D-glucopyranoside

N-methylaniline

Downstream raw materials:

methyl 3,4-di-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-O-(4-chlorobenzyl)-β-D-glucopyranoside

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