2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

Base Information

Chemical Name:2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine
CAS No.:1276019-47-6
Molecular Formula:C₅₃H₅₁N₃
Molecular Weight:730.008
Hs Code.:

Synonyms:2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

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Chemical Property of 2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

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Technology Process of 2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

There total 2 articles about 2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1276019-41-0
2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-acetylpyridine

: 24544-08-9
2,6-diethyl-4-methylaniline

: 1276019-47-6
2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Reflux;
DOI:10.1039/c0cc05373b

Reference yield:

: 1129-30-2
2,6-Diacetylpyridine

: 1276019-47-6
2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 6 h / Reflux

2: toluene-4-sulfonic acid / toluene / Reflux

With toluene-4-sulfonic acid; In toluene;
DOI:10.1039/c0cc05373b

Reference yield: 89.58%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 1276019-47-6
2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine

: 1357024-37-3
2-[1-(2,6-dibenzhydryl-4-methylphenylimino)ethyl]-6-[1-(2,6-diethyl-4-methylphenylimino)ethyl]pyridine NiCl₂

Guidance literature:: In dichloromethane; Ni complex and pyridine deriv. added to Schlenk tube with CH2Cl2; react.mixt. stirred for 8 h at room temp.; Et2O added; ppt. washed with Et2O; dried under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2011.12.031