(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

Base Information

Chemical Name:(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate
CAS No.:1388220-73-2
Molecular Formula:C₁₈H₂₇NO₆
Molecular Weight:353.415
Hs Code.:

Synonyms:(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

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Chemical Property of (S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

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Technology Process of (S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

There total 4 articles about (S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₅NO₆

: 1388220-73-2
(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.05.013

Reference yield:

: 626242-99-7
3-[4-(2-benzyloxy-ethoxy)-phenyl]-2-(tert-butoxycarbonyl-methyl-amino)-propionic acid methyl ester

: 1388220-73-2
(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 10h;
DOI:10.1055/s-0037-1610694

Reference yield:

: 147363-23-3
methyl (2S)-2-{[(tert-butoxy)carbonyl]amino}-3-[4-(prop-2-en-1-yloxy)phenyl]-propanoate

: 1388220-73-2
(S)-methyl 2-[tert-butoxycarbonyl(methyl)amino]-3-[4-(2-hydroxyethoxy)phenyl]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: silver(l) oxide / N,N-dimethyl-formamide / 9 h / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water; toluene / 4 h / 20 °C / Inert atmosphere

3: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; silver(l) oxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tetasy.2012.05.013