Technology Process of C28H24N2O6
There total 9 articles about C28H24N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H26N2O6;
With
water; lithium hydroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 4h;
With
hydrogenchloride;
In
tetrahydrofuran; water;
pH=3;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium hydroxide / methanol; water / Reflux
2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C
4.1: triethylamine / dichloromethane / 1 h / 0 °C
5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C
6.1: hydrazine hydrate / ethanol / 1 h / Reflux
7.1: water; ethyl acetate / 20 - 50 °C
8.1: 1,1'-carbonyldiimidazole / dichloromethane / 2 h / 20 - 25 °C
8.2: 20 - 25 °C
9.1: water; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C
9.2: pH 3
With
hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; 1,1'-carbonyldiimidazole; potassium iodide; sodium hydroxide; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: sodium hydroxide / methanol; water / Reflux
2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C
4.1: triethylamine / dichloromethane / 1 h / 0 °C
5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C
6.1: hydrazine hydrate / ethanol / 1 h / Reflux
7.1: water; ethyl acetate / 20 - 50 °C
8.1: 1,1'-carbonyldiimidazole / dichloromethane / 2 h / 20 - 25 °C
8.2: 20 - 25 °C
9.1: water; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C
9.2: pH 3
With
hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; 1,1'-carbonyldiimidazole; potassium iodide; sodium hydroxide; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;