(methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)

Base Information

Chemical Name:(methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)
CAS No.:771488-36-9
Molecular Formula:C₃₂H₂₈N₄Ni₂O₆S₄
Molecular Weight:810.242
Hs Code.:

Synonyms:(methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)

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Technology Process of (methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)

There total 1 articles about (methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3232-37-9,71112-98-6
salicylaldehyde benzoylhydrazone

: 2667-20-1
potassium methylxanthate

: 83864-14-6
nickel dichloride

: 771488-36-9
(methyl dithiocarbonate)(salicylaldehyde benzoylhydrazoneanion)nickel(II)

Guidance literature:: In ethanol; water; byproducts: KCl, HCl; salicylaldehyde benzoylhydrazone (1 equiv.) dissolved in abs. EtOH; added to NiCl2 in aq. EtOH; stirred for ca. 0.5 h; K alkyl dithiocarbonate (1 equiv.) in doubly distd. water added with stirring; filtered; ppt. washed with aq. EtOH; dried over P2O5; elem. anal.;
DOI:10.1081/SIM-120035954