N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

Base Information

Chemical Name:N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester
CAS No.:861632-15-7
Molecular Formula:C₁₇H₂₂N₂O₆S
Molecular Weight:382.437
Hs Code.:

Synonyms:N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

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Chemical Property of N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

Chemical Property:

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Technology Process of N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

There total 1 articles about N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 107-18-6
allyl alcohol

: 73270-67-4
(S)-2-allylamino-3-phenyl-propionic acid methyl ester

: 861632-15-7
N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

Guidance literature:: isocyanate de chlorosulfonyle; allyl alcohol; In dichloromethane; at 0 ℃; for 0.166667h;

(S)-2-allylamino-3-phenyl-propionic acid methyl ester; With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1016/j.tet.2005.03.140

Reference yield: 81.0%

: 861632-15-7
N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

: 100-51-6,185532-71-2
benzyl alcohol

: N-[[[(2-propenyloxy)carbonyl]-N'-(benzyl)amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.tet.2005.03.140

Reference yield:

: 861632-15-7
N-[[[(2-propenyloxy)carbonyl]amino]sulfonyl]-N-(2-propenyl)-(S)-phenylalanine methyl ester

: (2S)-2-(3-benzyl-2,4,4-trioxo-3,4,6,9-tetrahydro-2H-4λ⁶-[1,4,3,5]oxathiadiazonin-5-yl)-3-phenyl-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / DEAD; PPh₃ / tetrahydrofuran

2: 52 percent / (IMesH₂)(PCy₃)(Cl)2Ru=CHPh / CH₂Cl₂ / Heating

With triphenylphosphine; diethylazodicarboxylate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; dichloromethane; 1: Mitsunobu benzylation;
DOI:10.1016/j.tet.2005.03.140