C₅₃H₆₇FN₄O₉Si

Base Information

Chemical Name:C₅₃H₆₇FN₄O₉Si
CAS No.:1335557-72-6
Molecular Formula:C₅₃H₆₇FN₄O₉Si
Molecular Weight:951.22
Hs Code.:

C<sub>53</sub>H<sub>67</sub>FN<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₅₃H₆₇FN₄O₉Si

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Chemical Property of C₅₃H₆₇FN₄O₉Si

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Technology Process of C₅₃H₆₇FN₄O₉Si

There total 14 articles about C₅₃H₆₇FN₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335557-70-4
C₅₆H₇₁FN₄O₉Si

: 1335557-72-6
C₅₃H₆₇FN₄O₉Si

Guidance literature:: C₅₆H₇₁FN₄O₉Si; With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 394-04-7
5-fluoro-2-methoxybenzoic acid

: 1335557-72-6
C₅₃H₆₇FN₄O₉Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 2 h / -78 °C

1.2: 2 h / -78 - 25 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

2.2: 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

5.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

6.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

8.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

8.2: 0.5 h / -78 °C

8.3: -78 - 20 °C

9.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

11.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

12.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 5 h / 20 °C

13.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.55 h / -78 °C

13.2: 1 h / -78 - -20 °C

14.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 40 °C / Inert atmosphere

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; sec.-butyllithium; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexanes; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;

Reference yield:

: 220901-72-4
3-fluoro-6-methoxy-2-methylbenzoic acid

: 1335557-72-6
C₅₃H₆₇FN₄O₉Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 25 °C

1.2: 12 h / 25 °C

2.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

3.1: nitric acid; tetrabutylammomium bromide / water; 1,2-dichloro-ethane / 19 h / 20 - 26 °C

4.1: potassium carbonate; potassium iodide / acetone / 20 - 56 °C

5.1: water; sodium dithionite / tetrahydrofuran / 10 - 20.4 °C

6.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

7.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 0.58 h / -78 °C

7.2: 0.5 h / -78 °C

7.3: -78 - 20 °C

8.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

9.1: tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate / acetonitrile / 24 h / 70 °C

10.1: dmap; triethylamine; methanesulfonyl chloride / dichloromethane / 1 h / 20 °C

11.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 5 h / 20 °C

12.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.55 h / -78 °C

12.2: 1 h / -78 - -20 °C

13.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 24 h / 40 °C / Inert atmosphere

With dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; 1,3-dimethylbarbituric acid; N,N,N,N,-tetramethylethylenediamine; tetrabutylammomium bromide; water; nitric acid; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium tris(acetoxy)borohydride; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; diisopropylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexanes; hexane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;