C₉H₆Cl₂N₂O

Base Information

Chemical Name:C₉H₆Cl₂N₂O
CAS No.:1195951-56-4
Molecular Formula:C₉H₆Cl₂N₂O
Molecular Weight:229.065
Hs Code.:

C<sub>9</sub>H<sub>6</sub>Cl<sub>2</sub>N<sub>2</sub>O

Synonyms:C₉H₆Cl₂N₂O

Suppliers and Price of C₉H₆Cl₂N₂O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₉H₆Cl₂N₂O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₉H₆Cl₂N₂O

There total 1 articles about C₉H₆Cl₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6191-99-7,99471-66-6
(2E)-3-ethoxyprop-2-enoyl chloride

: 63352-99-8
(3,5-dichlorophenyl)hydrazine hydrochloride

: 1195951-56-4
C₉H₆Cl₂N₂O

Guidance literature:: (2E)-3-ethoxyprop-2-enoyl chloride; (3,5-dichlorophenyl)hydrazine hydrochloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 74h; Reflux;

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield: 78.0%

: 1195951-56-4
C₉H₆Cl₂N₂O

: 1195951-57-5
C₉H₅BrCl₂N₂O

Guidance literature:: With bromine; In tetrachloromethane; at 20 ℃; for 2.5h; Reflux;

Reference yield:

: 1195951-56-4
C₉H₆Cl₂N₂O

: 1195951-60-0
C₃₂H₃₃Cl₂N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / tetrachloromethane / 2.5 h / 20 °C / Reflux

2: pyridine; copper diacetate / 1,2-dichloro-ethane / 16 h / 20 °C / Molecular sieve

3: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,2-dimethoxyethane; water / 16 h / 100 °C

4: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

With pyridine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; bromine; copper diacetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrachloromethane; 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane;