Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester

Base Information

• Chemical Name: Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester
• CAS No.: 129748-83-0
• Molecular Formula: C₁₈H₂₅N₅O₄
• Molecular Weight: 375.428

Synonyms:Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester

Chemical Property of Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester

There total 3 articles about Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-phenyl-4,5-bis(hydroxymethyl)-1,2,3-triazole (51808-10-7) + Isopropyl isocyanate (1795-48-8) → Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester (129748-83-0)

Guidance literature:

With dmap; In dichloromethane; for 96h; Heating;

DOI:10.1002/jhet.5570270338

Reference yield:

1-phenyl-1H-[1,2,3]triazole-4,5-dicarboxylic acid dimethyl ester (17304-69-7) → Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester (129748-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / LiAlH₄ / diethyl ether / 12 h / Ambient temperature

2: 97 percent / 4-dimethylaminopyridine / CH₂Cl₂ / 96 h / Heating

With dmap; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;

DOI:10.1002/jhet.5570270338

Reference yield:

Phenyl azide (622-37-7) → Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester (129748-83-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 95 percent / CCl₄ / 12 h / Heating

2: 26 percent / LiAlH₄ / diethyl ether / 12 h / Ambient temperature

3: 97 percent / 4-dimethylaminopyridine / CH₂Cl₂ / 96 h / Heating

With dmap; lithium aluminium tetrahydride; In tetrachloromethane; diethyl ether; dichloromethane;

DOI:10.1002/jhet.5570270338

upstream raw materials:

1-phenyl-4,5-bis(hydroxymethyl)-1,2,3-triazole

Isopropyl isocyanate

1-phenyl-1H-[1,2,3]triazole-4,5-dicarboxylic acid dimethyl ester

Phenyl azide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 129748-83-0 Isopropyl-carbamic acid 5-isopropylcarbamoyloxymethyl-3-phenyl-3H-[1,2,3]triazol-4-ylmethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send