7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

Base Information

Chemical Name:7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide
CAS No.:1229648-53-6
Molecular Formula:C₂₉H₄₅NO₄Si
Molecular Weight:499.766
Hs Code.:

Synonyms:7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

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Technology Process of 7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

There total 1 articles about 7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1229648-52-5
6-[2-(tert-butyldiphenylsilanyloxy)pentyl]-4-methyltetrahydropyran-2-one

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1229648-53-6
7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

6-[2-(tert-butyldiphenylsilanyloxy)pentyl]-4-methyltetrahydropyran-2-one; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With water; rochelle salt; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/jo100443h

Reference yield: 88.0%

: 1229648-53-6
7-(tert-butyldiphenylsilanyloxy)-5-hydroxy-3-methyldecanoic acid N-methoxy-N-methylamide

: 420-37-1
trimethoxonium tetrafluoroborate

: 1229648-42-3
7-(tert-butyldiphenylsilanyloxy)-5-methoxy-3-methyldecanoic acid N-methoxy-N-methylamide

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere; Darkness; Molecular sieve;
DOI:10.1021/jo100443h