Technology Process of C66H85N11O15
There total 6 articles about C66H85N11O15 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-methyl-3-chloropyridinium iodide; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 16h;
DOI:10.1021/jo061918x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / HCTU; 6-chloro-1-hydroxy-1H-benzotriazole; 2,6-lutidine / CH2Cl2; dimethylformamide / 3.5 h
2: 89 percent / hydrogen / palladium on carbon / methanol / 16 h
3: 69 percent / 3-chloro-1-methylpyridinium iodide; ethyldiisopropylamine / CH2Cl2 / 16 h / 20 °C
With
2,6-dimethylpyridine; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); hydrogen; 1-methyl-3-chloropyridinium iodide; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo061918x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 89 percent / hydrogen / palladium on carbon / methanol / 16 h
2: 69 percent / 3-chloro-1-methylpyridinium iodide; ethyldiisopropylamine / CH2Cl2 / 16 h / 20 °C
With
hydrogen; 1-methyl-3-chloropyridinium iodide; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1021/jo061918x