N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide

Base Information

• Chemical Name: N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide
• CAS No.: 1038914-75-8
• Molecular Formula: C₂₇H₂₆N₂O₇S
• Molecular Weight: 522.579

Synonyms:N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide

Chemical Property of N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide

Chemical Property:

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Technology Process of N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide

There total 1 articles about N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

N-2-(1H-indol-3-yl)-2-oxoethyl-2-(3,4,5-trimethoxyphenyl)acetamide (953425-38-2) + benzenesulfonyl chloride (98-09-9) → N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide (1038914-75-8)

Guidance literature:

N-2-(1H-indol-3-yl)-2-oxoethyl-2-(3,4,5-trimethoxyphenyl)acetamide; With potassium hydroxide; In ethanol; at 50 ℃;

benzenesulfonyl chloride; In acetone; for 1h;

DOI:10.1021/jm8001185

Reference yield: 60.0%

N-[2-(1-phenylsulfonyl-1H-indol-3-yl)-2-oxoethyl]-2-(3,4,5-trimethoxyphenyl)acetamide (1038914-75-8) → 3-[1-(phenylsulfonyl)-1H-indol-3-yl]-4-(3,4,5-trimethoxyphenyl)-1H-pyrrole-2,5-dione (1038914-76-9)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; for 0.25h; Reflux;

DOI:10.1021/jm8001185

upstream raw materials:

N-2-(1H-indol-3-yl)-2-oxoethyl-2-(3,4,5-trimethoxyphenyl)acetamide

benzenesulfonyl chloride

Downstream raw materials:

3-[1-(phenylsulfonyl)-1H-indol-3-yl]-4-(3,4,5-trimethoxyphenyl)-1H-pyrrole-2,5-dione

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