N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

Base Information

Chemical Name:N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine
CAS No.:194285-51-3
Molecular Formula:C₁₈H₂₁Br₂N
Molecular Weight:411.179
Hs Code.:

Synonyms:N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

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Chemical Property of N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

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Technology Process of N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

There total 1 articles about N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-64-9
tert-butylamine

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 194285-51-3
N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.202011491

Reference yield: 59.0%

: 194285-51-3
N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

: 145434-22-6
2,4,6-triisopropylphenylboronic acid dimethyl ester

: C₃₃H₄₄BN

Guidance literature:: N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine; With n-butyllithium; In diethyl ether; hexane; at -30 ℃; for 1h; Inert atmosphere;

2,4,6-triisopropylphenylboronic acid dimethyl ester; In diethyl ether; hexane; at 0 - 20 ℃; for 14h; Inert atmosphere; Reflux;
DOI:10.1021/acs.orglett.8b02774

Reference yield:

: 194285-51-3
N,N -bis(2-bromobenzyl)-2-methylpropan-2-amine

: 363622-47-3
12-phenyl-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azabismocine

Guidance literature:: Multi-step reaction with 2 steps

1: n-C₄H₉Li / hexane; diethyl ether

2: diethyl ether; cyclohexane

With n-C₄H₉Li; In diethyl ether; hexane; cyclohexane;
DOI:10.1016/j.jorganchem.2004.06.041