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2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime

Base Information
  • Chemical Name:2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime
  • CAS No.:183657-32-1
  • Molecular Formula:C9H10N2O4
  • Molecular Weight:210.189
  • Hs Code.:
2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime

Synonyms:2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime

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Chemical Property of 2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime
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Technology Process of 2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime

There total 1 articles about 2-(2-Methoxy-phenyl)-1-nitro-ethanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydroxide; sodium nitrite; In methanol; at 0 ℃;
DOI:10.1016/0040-4039(96)01779-0
Guidance literature:
With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1016/0040-4039(96)01779-0
Guidance literature:
Multi-step reaction with 2 steps
1: 93 percent / Et3N / CH2Cl2 / Ambient temperature
2: 100 percent / Bu3SnH, AIBN / benzene / Heating
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; In dichloromethane; benzene;
DOI:10.1016/0040-4039(96)01779-0
upstream raw materials:

1-methoxy-2-(2-nitroethyl)benzene

Downstream raw materials:

C22H18N2O5

2-methoxy-benzeneacetonitrile

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