methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

Base Information

Chemical Name:methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate
CAS No.:1416900-81-6
Molecular Formula:C₁₉H₉Cl₃F₇N₃O₂
Molecular Weight:550.647
Hs Code.:

Synonyms:methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

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Chemical Property of methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

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Technology Process of methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

There total 4 articles about methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 792912-10-8
2-chloro-5-ethynyl-benzoic acid methyl ester

: 1334128-68-5
2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene

: 1416900-81-6
methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; for 96h;

Reference yield:

: 251085-87-7
methyl 5-bromo-2-chloro-benzoate

: 1416900-81-6
methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / triphenylphosphine; palladium diacetate / Inert atmosphere; Reflux

2: potassium carbonate; methanol / tetrahydrofuran / 1 h

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

With methanol; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; triethylamine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; water; tert-butyl alcohol;

Reference yield:

: 792911-91-2
methyl 2-chloro-5-((trimethylsilyl)ethynyl)benzoate

: 1416900-81-6
methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; methanol / tetrahydrofuran / 1 h

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h

With methanol; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol;