Technology Process of C35H33N2O4P
There total 4 articles about C35H33N2O4P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium borohydride / tetrahydrofuran; ethanol / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2.25 h / -60 °C
3.1: trichlorophosphate / acetonitrile / 6 h / Reflux
3.2: 4 h / Reflux
4.1: palladium 10% on activated carbon; hydrogen / methanol
With
lithium borohydride; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; dimethyl sulfoxide; trichlorophosphate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile;
2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1016/j.bmcl.2012.07.011
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trichlorophosphate / acetonitrile / 6 h / Reflux
1.2: 4 h / Reflux
2.1: palladium 10% on activated carbon; hydrogen / methanol
With
palladium 10% on activated carbon; hydrogen; trichlorophosphate;
In
methanol; acetonitrile;
DOI:10.1016/j.bmcl.2012.07.011