9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

Base Information

Chemical Name:9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole
CAS No.:148582-31-4
Molecular Formula:C₃₀H₂₇N₃O₃
Molecular Weight:477.563
Hs Code.:

Synonyms:9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

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Chemical Property of 9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

Chemical Property:

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Technology Process of 9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

There total 5 articles about 9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1477-55-0
1,3-di(aminomethyl)benzene

: 148582-31-4
9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 9 percent / CH₂Cl₂ / 12 h

2: 1.) carbonyldiimidazole (CDI) / 1.) THF, 1 h, 2.) THF, 1.5 h

With 1,1'-carbonyldiimidazole; In dichloromethane;
DOI:10.1021/ja00062a020

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 148582-31-4
9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃ / 1.) DMF, 50 deg C, 45 min, 2.) DMF, 50 deg C, 14 h

2: 96 percent / 1 N KOH / methanol / 0.83 h

3: 1.) carbonyldiimidazole (CDI) / 1.) THF, 1 h, 2.) THF, 1.5 h

With potassium hydroxide; potassium carbonate; 1,1'-carbonyldiimidazole; In methanol;
DOI:10.1021/ja00062a020

Reference yield:

: 143948-85-0
N-((methoxycarbonyl)methyl)carbazole

: 148582-31-4
9-<(((3-((((benzyloxy)carbonyl)amino)methyl)benzyl)amino)carbonyl)methyl>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1 N KOH / methanol / 0.83 h

2: 1.) carbonyldiimidazole (CDI) / 1.) THF, 1 h, 2.) THF, 1.5 h

With potassium hydroxide; 1,1'-carbonyldiimidazole; In methanol;
DOI:10.1021/ja00062a020