2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

Base Information

Chemical Name:2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene
CAS No.:1614246-71-7
Molecular Formula:C₂₄H₂₀BFN₂O₂S
Molecular Weight:430.31
Hs Code.:

Synonyms:2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

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Chemical Property of 2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

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Technology Process of 2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

There total 3 articles about 2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1338697-45-2
3-chloro-4-fluoro-1-(2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborinyl)benzene

: 352530-24-6
4-(ethylsulfonyl)phenylboronic acid

: 1614246-71-7
2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate tribasic; In N,N-dimethyl-formamide; at 100 ℃; for 12h; Inert atmosphere;

Reference yield:

: 144432-85-9
3-chloro-4-fluorophenylboronic acid

: 1614246-71-7
2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate tribasic; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate tribasic; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/acs.jmedchem.9b00322

Reference yield:

: 144432-85-9
3-chloro-4-fluorophenylboronic acid

: 479-27-6
naphthalene-1,8-diamine

: 1614246-71-7
2-(4'-ethylsulfonyl-6-fluorobiphenyl-3-yl)-2,3-dihydro-1H-1,3-diaza-2-boraphenalene

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / Reflux

2: potassium phosphate tribasic; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate tribasic; In N,N-dimethyl-formamide; toluene;