Technology Process of C23H26N4O6
There total 7 articles about C23H26N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / toluene / 26 h / 110 °C / Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 12 h / 23 °C / Inert atmosphere
3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 23 °C / Inert atmosphere
4: sodium azide / water; acetone / 1 h / 0 °C
With
sodium azide; oxalyl dichloride; triethylamine; trifluoroacetic acid;
N,N-dimethyl-formamide;
In
dichloromethane; water; acetone; toluene;
- Guidance literature:
-
With
sodium azide;
In
water; acetone;
at 0 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / ethanol / 12 h / 23 °C / Inert atmosphere
2.1: zinc; ammonium chloride / water; tetrahydrofuran / 1 h / 50 °C / Inert atmosphere
2.2: 0.17 h / 23 °C / Inert atmosphere
3.1: triethylamine / toluene / 26 h / 110 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 12 h / 23 °C / Inert atmosphere
5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0 - 23 °C / Inert atmosphere
6.1: sodium azide / water; acetone / 1 h / 0 °C
With
sodium azide; oxalyl dichloride; ammonium chloride; triethylamine; trifluoroacetic acid; zinc;
N,N-dimethyl-formamide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone; toluene;