(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

Base Information

Chemical Name:(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid
CAS No.:1197396-46-5
Molecular Formula:C₂₃H₂₇NO₇
Molecular Weight:429.47
Hs Code.:

Synonyms:(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

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Chemical Property of (1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

Chemical Property:

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Technology Process of (1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

There total 4 articles about (1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₅NO₇

: 1197396-46-5
(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 12h; Inert atmosphere;

Reference yield:

: 85-44-9
phthalic anhydride

: 1197396-46-5
(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene / 26 h / 110 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 12 h / 23 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane; toluene;

Reference yield:

: 1141364-91-1
(1S,2R,3S,4R,5S)-4-tert-butyl-1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate

: 1197396-46-5
(1R,2R,6S)-6-(1,3-dioxoisoindolin-2-yl)-4-(ethoxycarbonyl)-2-(3-pentyloxy)cyclohex-3-enecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc; ammonium chloride / water; tetrahydrofuran / 1 h / 50 °C / Inert atmosphere

1.2: 0.17 h / 23 °C / Inert atmosphere

2.1: triethylamine / toluene / 26 h / 110 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 12 h / 23 °C / Inert atmosphere

With ammonium chloride; triethylamine; trifluoroacetic acid; zinc; In tetrahydrofuran; dichloromethane; water; toluene;