(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester
CAS No.:1027635-92-2
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

Synonyms:(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of (3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of (3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

There total 4 articles about (3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1027635-96-6
5-allyloxymethyl-benzene-1,3-diamine

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1027635-92-2
(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,2-dioxacyclohexane; at 20 ℃; for 2h;
DOI:10.1021/jm200326p

Reference yield:

: 1027635-96-6
5-allyloxymethyl-benzene-1,3-diamine

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1027635-92-2
(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

: C₄₀H₃₄N₂O₅

Guidance literature:: 5-allyloxymethyl-benzene-1,3-diamine; (fluorenylmethoxy)carbonyl chloride; In dichloromethane; for 0.0833333h;

With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

Reference yield:

: 71022-43-0
3,5-dinitrobenzyl alcohol

: 1027635-92-2
(3-allyloxymethyl-5-aminophenyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / 12 h / 20 °C

2: iron; ammonium chloride / ethanol; water / 4 h / 50 - 80 °C

3: N-ethyl-N,N-diisopropylamine / 1,2-dioxacyclohexane / 2 h / 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,2-dioxacyclohexane; ethanol; water;
DOI:10.1021/jm200326p