1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

Base Information

Chemical Name:1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide
CAS No.:132680-27-4
Molecular Formula:C₁₈H₁₈N₄O
Molecular Weight:306.367
Hs Code.:

Synonyms:1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

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Chemical Property of 1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

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Technology Process of 1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

There total 3 articles about 1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123-75-1
pyrrolidine

: 132680-71-8
1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid

: 132680-27-4
1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1002/jhet.5570270653

Reference yield:

: 132680-70-7
1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid ethyl ester

: 132680-27-4
1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 10percent KOH / ethanol / 1.25 h / Heating

2: 90 percent / N-(dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride, triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

With potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/jhet.5570270653

Reference yield:

: 16078-63-0
3-amino-1-phenyl-1H-pyrazole-4-carboxylic acid ethyl ester

: 132680-27-4
1-phenyl-3-(1H-pyrrol-1-yl)-1H-pyrazole-4-carboxylic acid pyrrolidinamide

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / glacial acetic acid / 0.5 h / Heating

2: 97 percent / 10percent KOH / ethanol / 1.25 h / Heating

3: 90 percent / N-(dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride, triethylamine / CH₂Cl₂ / 20 h / Ambient temperature

With potassium hydroxide; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/jhet.5570270653