dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Base Information

Chemical Name:dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate
CAS No.:226919-64-8
Molecular Formula:C₄₀H₅₅O₁₀P
Molecular Weight:726.844
Hs Code.:

Synonyms:dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Suppliers and Price of dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

There total 5 articles about dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphoric acid (3R,4R,5S,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-hydroxy-tetrahydro-pyran-2-yl ester dibutyl ester

: 3282-30-2
pivaloyl chloride

: dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-α-D-galactopyranoside phosphate

: 226919-64-8
dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1021/ja016227r

Reference yield:

: (3R,4S,5S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2,7-dioxa-bicyclo[4.1.0]heptane

: 226919-64-8
dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / -78 °C

2: DMAP / CH₂Cl₂ / 1 h / 20 °C

With dmap; In dichloromethane;
DOI:10.1021/ol9905452

Reference yield:

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 226919-64-8
dibutyl 2-O-pivaloyl-3,4,6-tri-O-benzyl-β-D-galactopyranoside phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl dioxirane / CH₂Cl₂; acetone / 0.25 h / 0 °C

2: CH₂Cl₂ / -78 °C

3: DMAP / CH₂Cl₂ / 1 h / 20 °C

With dmap; 3,3-dimethyldioxirane; In dichloromethane; acetone;
DOI:10.1021/ol9905452