(E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

Base Information

Chemical Name:(E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide
CAS No.:1361032-08-7
Molecular Formula:C₁₇H₂₃NO₂S
Molecular Weight:305.441
Hs Code.:

Synonyms:(E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

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Technology Process of (E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

There total 1 articles about (E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 32364-41-3
1-tosyloxy-1-vinylcyclopropane

: 86410-99-3
N-<(E)-2-methyl-2-butenyl>-p-tosylamide

: 1361032-08-7
(E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

Guidance literature:: N-<(E)-2-methyl-2-butenyl>-p-tosylamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

1-tosyloxy-1-vinylcyclopropane; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,2-bis-(diphenylphosphino)ethane; In tetrahydrofuran; mineral oil; at 20 ℃; for 16.5h; Inert atmosphere;
DOI:10.1021/ja210804r

Reference yield: 84.0%

: 1361032-08-7
(E)-N-(2-cyclopropylideneethyl)-4-methyl-N-(2-methylbut-2-enyl)benzene sulfonamide

: (3RS,4SR)-3-methyl-4-(prop-1-en-2-yl)-1-tosyl-3-vinylpyrrolidine

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-p-tolylphosphite; In toluene; at 100 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja210804r