C₃₆H₄₄N₂O₉

Base Information

Chemical Name:C₃₆H₄₄N₂O₉
CAS No.:1308253-72-6
Molecular Formula:C₃₆H₄₄N₂O₉
Molecular Weight:648.753
Hs Code.:

C<sub>36</sub>H<sub>44</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₆H₄₄N₂O₉

Suppliers and Price of C₃₆H₄₄N₂O₉

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₄₄N₂O₉

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₄₄N₂O₉

There total 12 articles about C₃₆H₄₄N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1308253-75-9
C₄₈H₇₂N₂O₉Si₂

: 1308253-72-6
C₃₆H₄₄N₂O₉

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/jhet.609

Reference yield:

: 1177255-27-4
(S)-methyl-2-acetamido-3-(3-formyl-4-methoxy-3-methylphenyl)propanoate

: 1308253-72-6
C₃₆H₄₄N₂O₉

Guidance literature:: Multi-step reaction with 10 steps

1: 3-chloro-benzenecarboperoxoic acid / chloroform / 6 h / 20 °C

2: hydrogenchloride; water / methanol / 10 h

3: lithium borohydride / tetrahydrofuran / 24 h

4: hydrogenchloride / methanol; water / 6 h / Reflux

5: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

6: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

7: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

8: formic acid / tetrahydrofuran; water / 2 h / 20 °C

9: Dess-Martin periodane / dichloromethane / 0 - 20 °C

10: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; lithium borohydride; formic acid; tetrabutyl ammonium fluoride; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; 2,2,2-trifluoroethanol; water; 1: Baeyer-Villiger oxidation;
DOI:10.1002/jhet.609

Reference yield:

: 1177255-28-5
(S)-methyl-2-acetamido-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

: 1308253-72-6
C₃₆H₄₄N₂O₉

Guidance literature:: Multi-step reaction with 8 steps

1: lithium borohydride / tetrahydrofuran / 24 h

2: hydrogenchloride / methanol; water / 6 h / Reflux

3: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

5: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

6: formic acid / tetrahydrofuran; water / 2 h / 20 °C

7: Dess-Martin periodane / dichloromethane / 0 - 20 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; lithium borohydride; formic acid; tetrabutyl ammonium fluoride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; Dess-Martin periodane; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1002/jhet.609