Technology Process of C21H29NO3S
There total 6 articles about C21H29NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thallium(I) carbonate; dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll);
In
tetrahydrofuran; water;
at 50 ℃;
DOI:10.1002/chem.201201332
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium perchlorate / acetone / 48 h / 40 °C / Inert atmosphere
2.1: sodium hydroxide / water; tert-butyl alcohol / 1 h / 25 °C / Inert atmosphere
2.2: 25 °C / Inert atmosphere
3.1: dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); thallium(I) carbonate / water; tetrahydrofuran / 50 °C
With
thallium(I) carbonate; dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); sodium perchlorate; sodium hydroxide;
In
tetrahydrofuran; water; acetone; tert-butyl alcohol;
3.1: |Suzuki Coupling;
DOI:10.1002/chem.201201332
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide / water; tert-butyl alcohol / 1 h / 25 °C / Inert atmosphere
1.2: 25 °C / Inert atmosphere
2.1: dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); thallium(I) carbonate / water; tetrahydrofuran / 50 °C
With
thallium(I) carbonate; dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); sodium hydroxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
2.1: |Suzuki Coupling;
DOI:10.1002/chem.201201332