1-(4-(tert-butylthio)phenyl)ethan-1-one

Base Information

Chemical Name:1-(4-(tert-butylthio)phenyl)ethan-1-one
CAS No.:4074-62-8
Molecular Formula:C₁₂H₁₆OS
Molecular Weight:208.324
Hs Code.:

Synonyms:1-(4-(tert-butylthio)phenyl)ethan-1-one

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Chemical Property of 1-(4-(tert-butylthio)phenyl)ethan-1-one

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Technology Process of 1-(4-(tert-butylthio)phenyl)ethan-1-one

There total 7 articles about 1-(4-(tert-butylthio)phenyl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 99-90-1
para-bromoacetophenone

: 75-66-1
2-methylpropan-2-thiol

: 4074-62-8
1-(4-(tert-butylthio)phenyl)ethan-1-one

Guidance literature:: With C₃₀H₃₂Cl₃N₄Ni₂⁽¹⁺⁾*Cl^(1-); potassium hydroxide; In 1,4-dioxane; at 40 ℃; for 6h; Reagent/catalyst;
DOI:10.1021/acs.organomet.0c00732

Reference yield: 78.0%

: 127-19-5,116057-81-9
N,N-dimethyl acetamide

: 25752-90-3
tert-butyl 4-bromophenyl sulfide

: 4074-62-8
1-(4-(tert-butylthio)phenyl)ethan-1-one

Guidance literature:: tert-butyl 4-bromophenyl sulfide; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.25h;

N,N-dimethyl acetamide; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 0.5h;
DOI:10.1021/jo400362u

Reference yield: 70.0%

: indium tris(tert-butylthiolate)

: 99-91-2
para-chloroacetophenone

: 4074-62-8
1-(4-(tert-butylthio)phenyl)ethan-1-one

Guidance literature:: para-chloroacetophenone; With palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;

indium tris(tert-butylthiolate); With caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1246/cl.2011.980