2-Azido-1-iodo-3-phenylpropan

Base Information

• Chemical Name: 2-Azido-1-iodo-3-phenylpropan
• CAS No.: 16484-04-1
• Molecular Formula: C₉H₁₀IN₃
• Molecular Weight: 287.103
• Mol file: 16484-04-1.mol

Synonyms:2-Azido-1-iodo-3-phenylpropan

Chemical Property of 2-Azido-1-iodo-3-phenylpropan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-Azido-1-iodo-3-phenylpropan

There total 1 articles about 2-Azido-1-iodo-3-phenylpropan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allylbenzene (300-57-2,57807-91-7) → 2-Azido-1-iodo-3-phenylpropan (16484-04-1)

Guidance literature:

With iodine(I) azide; In acetonitrile;

DOI:10.1021/ja00985a019

Reference yield:

2-Azido-1-iodo-3-phenylpropan (16484-04-1) → (2-azidoallyl)benzene (28022-22-2)

Guidance literature:

With potassium tert-butylate;

DOI:10.1016/S0040-4039(00)90998-5

Reference yield:

2-Azido-1-iodo-3-phenylpropan (16484-04-1) + 4-nitro-benzoyl chloride (122-04-3) → 4-nitro-N-(β-methylphenethyl)benzamide (15269-43-9)

Guidance literature:

Multistep reaction; (i) LiAlH₄, Et₂O, (ii) /BRN= 473192/, Et₃N, benzene;

DOI:10.1021/ja01046a019

upstream raw materials:

allylbenzene

Downstream raw materials:

(2-azidoallyl)benzene

4-nitro-N-(β-methylphenethyl)benzamide