(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Base Information

Chemical Name:(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate
CAS No.:881920-71-4
Molecular Formula:C₁₇H₃₃NO₂Si
Molecular Weight:311.54
Hs Code.:

Synonyms:(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Suppliers and Price of (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

There total 4 articles about (S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2,2,2-Trichloro-acetyl)-carbamic acid (E)-(S)-1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-3-trimethylsilanyl-allyl ester

: 881920-71-4
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Guidance literature:: With potassium carbonate; In methanol; water; at 0 - 23 ℃;
DOI:10.1021/ol053061g

Reference yield:

: 881920-65-6
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)prop-2-en-1-ol

: 881920-71-4
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 1 h / 0 °C

2: 987 mg / potassium carbonate / methanol; H₂O / 0 - 23 °C

With potassium carbonate; In methanol; dichloromethane; water;
DOI:10.1021/ol053061g

Reference yield:

: 70737-22-3
((E)-2-iodoethenyl)(trimethyl)silane

: 881920-71-4
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-(trimethylsilyl)allyl carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert-butyllithium / diethyl ether; pentane / -78 - 23 °C

1.2: 40 percent / diethyl ether; pentane / 3 h / -78 °C

2.1: CH₂Cl₂ / 1 h / 0 °C

3.1: 987 mg / potassium carbonate / methanol; H₂O / 0 - 23 °C

With tert.-butyl lithium; potassium carbonate; In methanol; diethyl ether; dichloromethane; water; pentane;
DOI:10.1021/ol053061g