(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Base Information

Chemical Name:(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate
CAS No.:1456693-00-7
Molecular Formula:C₁₇H₂₆N₂O₅
Molecular Weight:338.404
Hs Code.:
Mol file:1456693-00-7.mol

Synonyms:(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Suppliers and Price of (R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of (R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of (R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

There total 1 articles about (R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

: 1685-33-2
N-[(benzyloxy)carbonyl]-D-valine

: 22483-09-6
2,2-dimethoxyethylamine

: 1456693-00-7
(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: N-[(benzyloxy)carbonyl]-D-valine; With 4-methyl-morpholine; isobutyl chlorocarbonate; In tetrahydrofuran; at -15 ℃; for 0.5h;

2,2-dimethoxyethylamine; In tetrahydrofuran; at -15 ℃; for 2h;

Reference yield: 95.4%

: 1456693-00-7
(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

: 1456693-01-8
(R)-benzyl 2-isopropyl-3-oxo-3,4-dihydropyrazine-1(2H)-carboxylate

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 12h;

Reference yield:

: 1456693-00-7
(R)-benzyl (1-((2,2-dimethoxyethyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

: 1456693-04-1
(R)-tert-butyl 4-(5-fluoro-4-(methoxycarbonyl)-2-nitrophenyl)-2-isopropyl-3-oxopiperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / 12 h / 20 °C

2.1: triethylsilane / 1,2-dichloro-ethane / 36 h / 20 °C / Reflux

3.1: 15% palladium on carbon; hydrogen / methanol / 20 °C

4.1: 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / -10 °C / Inert atmosphere

5.2: 0.33 h / -30 - -20 °C

With triethylsilane; 15% palladium on carbon; hydrogen; sodium hydride; trifluoroacetic acid; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;