2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

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Chemical Name:2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate
CAS No.:1402555-57-0
Molecular Formula:C₂₇H₃₆ClN₅O₁₂
Molecular Weight:658.062
Hs Code.:

Synonyms:2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

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Chemical Property of 2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

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Technology Process of 2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

There total 7 articles about 2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 74124-79-1
di(succinimido) carbonate

: 1402555-56-9
1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaocta-triazaoctadecan-18-oic acid

: 1402555-57-0
2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

Guidance literature:: With pyridine; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1185730-50-0
methyl 6-((3-(4,5-dimethoxy-2-nitrophenyl)-3-hydroxypropyl)(methyl)amino)-6-oxohexanoate

: 1402555-57-0
2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 3 h / 20 °C / Inert atmosphere

2: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

4: water; lithium hydroxide / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

5: pyridine / acetonitrile / 16 h / 20 °C / Inert atmosphere

With pyridine; water; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/anie.201201690

Reference yield:

: 1185730-61-3
C₂₃H₃₀N₄O₉

: 1402555-57-0
2,5-dioxopyrrolidin-1-yl 1-chloro-9-(4,5-dimethoxy-2-nitrophenyl)-12-methyl-2,7,13-trioxo-8-oxa-3,6,12-triazaoctadecan-18-oate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

3: water; lithium hydroxide / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4: pyridine / acetonitrile / 16 h / 20 °C / Inert atmosphere

With pyridine; water; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/anie.201201690