C₃₄H₂₅N₅O₂Zn

Base Information

• Chemical Name: C₃₄H₂₅N₅O₂Zn
• CAS No.: 1400683-72-8
• Molecular Formula: C₃₄H₂₅N₅O₂Zn
• Molecular Weight: 600.995
• Mol file: 1400683-72-8.mol

Synonyms:C₃₄H₂₅N₅O₂Zn

Chemical Property of C₃₄H₂₅N₅O₂Zn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₅N₅O₂Zn

There total 4 articles about C₃₄H₂₅N₅O₂Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

sodium tetrahydroborate (16940-66-2) + C22H16BrN3O3 (1400683-63-7) + zinc diacetate (557-34-6) + 2-[(3,3,5-trimethyl-3,4-dihydro-2H-pyrrol-2-yl)methyl]pyrrole (276239-53-3) → C34H25N5O2Zn (1400683-72-8)

Guidance literature:

sodium tetrahydroborate; C₂₂H₁₆BrN₃O₃; With methanol; In tetrahydrofuran; for 0.75h; Cooling with ice;

2-[(3,3,5-trimethyl-3,4-dihydro-2H-pyrrol-2-yl)methyl]pyrrole; With trifluoroacetic acid; In acetonitrile; for 0.5h;

zinc diacetate; With 2,2,6,6-tetramethyl-piperidine; silver trifluoromethanesulfonate; In acetonitrile; at 85 ℃; for 24h;

DOI:10.1021/ic3015354

Reference yield:

4-nitro-benzoyl chloride (122-04-3) → C34H25N5O2Zn (1400683-72-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: isopropylmagnesium bromide / tetrahydrofuran; toluene / 0.33 h / Inert atmosphere; Cooling with ice

1.2: 1 h / -78 - 20 °C / Inert atmosphere

2.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / -78 °C

3.1: methanol / tetrahydrofuran / 0.75 h / Cooling with ice

3.2: 0.5 h

3.3: air / 24 h / 85 °C

With methanol; N-Bromosuccinimide; isopropylmagnesium bromide; In tetrahydrofuran; toluene;

DOI:10.1021/ic3015354

Reference yield:

C22H17N3O3 (1400683-62-6) → C34H25N5O2Zn (1400683-72-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / -78 °C

2.1: methanol / tetrahydrofuran / 0.75 h / Cooling with ice

2.2: 0.5 h

2.3: air / 24 h / 85 °C

With methanol; N-Bromosuccinimide; In tetrahydrofuran;

DOI:10.1021/ic3015354

upstream raw materials:

sodium tetrahydroborate

C₂₂H₁₆BrN₃O₃

zinc diacetate

2-[(3,3,5-trimethyl-3,4-dihydro-2H-pyrrol-2-yl)methyl]pyrrole

Downstream raw materials:

C₃₆H₂₉N₅OZn