5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

Base Information

Chemical Name:5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin
CAS No.:325708-61-0
Molecular Formula:C₁₆H₁₈N₆O₆
Molecular Weight:390.356
Hs Code.:

Synonyms:5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

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Chemical Property of 5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

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Technology Process of 5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

There total 2 articles about 5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 88091-68-3
2-(4-nitrophenyl)ethoxycarbonyl chloride

: 31969-10-5
6-hydroxymethyl-5,6,7,8-tetrahydropterin dihydrochloride

: 325708-61-0
5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1002/1522-2675(20001004)83:10<2738::AID-HLCA2738>3.0.CO;2-A

Reference yield:

: 712-29-8
6-(hydroxymethyl)pterin

: 325708-61-0
5,6,7,8-tetrahydro-6-(hydroxymethyl)-5-{[2-(4-nitrophenyl)ethoxy]carbonyl}pterin

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / trifluoroacetic acid / 4 h / 20 °C

2: 86 percent / pyridine / 12 h / 20 °C

With pyridine; hydrogen; platinum(IV) oxide; In trifluoroacetic acid; 1: Hydrogenation / 2: Acylation;
DOI:10.1002/1522-2675(20001004)83:10<2738::AID-HLCA2738>3.0.CO;2-A