6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

Base Information

Chemical Name:6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside
CAS No.:74653-40-0
Molecular Formula:C₃₅H₅₀N₂O₁₃
Molecular Weight:706.788
Hs Code.:

Synonyms:6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

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Chemical Property of 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

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Technology Process of 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

There total 7 articles about 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 74653-39-7
Acetic acid (2R,3S,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-[(2R,3S,4R,5R,6R)-5-acetylamino-4-benzyloxy-6-(6-benzyloxycarbonylamino-hexyloxy)-3-hydroxy-tetrahydro-pyran-2-ylmethoxy]-tetrahydro-pyran-4-yl ester

: 74653-40-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; for 1h;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

: 74653-40-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

2: 1.) BaO-Ba(OH)2*8H₂O; 2.) acetic acid / 1.) DMF, 0 deg C, 4 h; 2.) 10 h, 55 deg C

3: 66 percent / silver trifluoromethanesulfonate / CH₂Cl₂ / 2 h / 0 °C

4: 94 percent / sodium methoxide / methanol / 1 h

With barium dihydroxide; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; barium(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 62205-56-5,159173-77-0
6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside

: 74653-40-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-6-O-β-D-galactopyranosyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / sodium methoxide / methanol / 24 h

2: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

3: 1.) BaO-Ba(OH)2*8H₂O; 2.) acetic acid / 1.) DMF, 0 deg C, 4 h; 2.) 10 h, 55 deg C

4: 66 percent / silver trifluoromethanesulfonate / CH₂Cl₂ / 2 h / 0 °C

5: 94 percent / sodium methoxide / methanol / 1 h

With barium dihydroxide; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; barium(II) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85520-2