(6R,7S,9R)-7-hydroxy-α-dihydroionol

Base Information

Chemical Name:(6R,7S,9R)-7-hydroxy-α-dihydroionol
CAS No.:908297-92-7
Molecular Formula:C₁₃H₂₄O₂
Molecular Weight:212.332
Hs Code.:

Synonyms:(6R,7S,9R)-7-hydroxy-α-dihydroionol

Suppliers and Price of (6R,7S,9R)-7-hydroxy-α-dihydroionol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (6R,7S,9R)-7-hydroxy-α-dihydroionol

Chemical Property:

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Technology Process of (6R,7S,9R)-7-hydroxy-α-dihydroionol

There total 5 articles about (6R,7S,9R)-7-hydroxy-α-dihydroionol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: (6RS,7SR,9RS)-7-hydroxy-α-dihydroionol

: 108-05-4,9003-20-7
vinyl acetate

: (6S,7R,9S)-7-hydroxy-α-dihydroionol

: 908297-92-7
(6R,7S,9R)-7-hydroxy-α-dihydroionol

: 143679-50-9
(-)-(6S,7R,9S)-7-hydroxy-α-dihydroionol acetate

Guidance literature:: With Pseudomonas cepacia lipase PS; In various solvent(s); at 20 ℃; for 144h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2006.05.024

Reference yield:

: 908297-94-9
Acetic acid (1S,3R)-3-acetoxy-1-((R)-2,6,6-trimethyl-cyclohex-2-enyl)-butyl ester

: 908297-92-7
(6R,7S,9R)-7-hydroxy-α-dihydroionol

Guidance literature:: With potassium hydroxide; In methanol;
DOI:10.1016/j.tetasy.2006.05.024

Reference yield:

: (6RS,7SR)-7-hydroxy-α-dihydroionone

: 908297-92-7
(6R,7S,9R)-7-hydroxy-α-dihydroionol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 15 h / -10 °C

2: Pseudomonas cepacia lipase PS / various solvent(s) / 144 h / 20 °C

With Pseudomonas cepacia lipase PS; acetic acid; tetramethylammonium triacetoxyborohydride; In acetonitrile;
DOI:10.1016/j.tetasy.2006.05.024