1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

Base Information

Chemical Name:1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate
CAS No.:1264635-62-2
Molecular Formula:C₁₉H₁₉Cl₂NO₅
Molecular Weight:412.27
Hs Code.:

Synonyms:1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

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Chemical Property of 1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

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Technology Process of 1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

There total 2 articles about 1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 258841-42-8
isopropyloxycarbonyloxymethyl iodide

: 15307-79-6
diclofenac sodium

: 1264635-62-2
1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

Guidance literature:: diclofenac sodium; With sodium carbonate; In N,N-dimethyl acetamide; at 30 ℃; for 0.166667h; Inert atmosphere;

isopropyloxycarbonyloxymethyl iodide; In N,N-dimethyl acetamide; at -10 ℃; for 0.75h; Inert atmosphere;
DOI:10.1021/jm101095e

Reference yield:

: 35180-01-9
chloromethyl isopropyl carbonate

: 1264635-62-2
1-[(1-methylethoxy)carbonyloxy]methyl 2-[(2,6-dichlorophenyl)amino]phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide / acetonitrile / 22 h / 30 °C / Inert atmosphere

2.1: sodium carbonate / N,N-dimethyl acetamide / 0.17 h / 30 °C / Inert atmosphere

2.2: 0.75 h / -10 °C / Inert atmosphere

With sodium carbonate; sodium iodide; In N,N-dimethyl acetamide; acetonitrile;
DOI:10.1021/jm101095e