dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

Base Information

Chemical Name:dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate
CAS No.:1059116-18-5
Molecular Formula:C₅₀H₅₅O₁₂P
Molecular Weight:878.953
Hs Code.:

Synonyms:dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

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Chemical Property of dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

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Technology Process of dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

There total 1 articles about dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059116-10-7
dibutyl (2-O-benzoyl-3,4-di-O-benzyl-α-D-mannopyranosyl) phosphate

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1059116-18-5
dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/b804069a

Reference yield: 80.0%

: 1059116-18-5
dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

: C₁₆₇H₁₆₆O₃₇

Guidance literature:: dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -15 ℃; Automated synthesizer; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; Automated synthesizer; solid phase reaction;

dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate; Further stages;
DOI:10.1039/b804069a

Reference yield: 57.0%

: 1059116-18-5
dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate

: C₂₁H₂₅N₂O₆Pol

: C₉₄H₉₇NO₂₁

Guidance literature:: dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate; C₂₁H₂₅N₂O₆Pol; With trimethylsilyl trifluoromethanesulfonate; In chloroform; at -10 - 20 ℃; under 7875.79 Torr; not specified Inert atmosphere; Flow reactor;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 20 ℃; under 7875.79 Torr; not specified Inert atmosphere; Flow reactor;

dibutyl 2-O-benzoyl-3,4-di-O-benzyl-6-O-(9-fluorenylmethoxycarbonyl)-α-D-mannopyranosyl phosphate; Further stages;
DOI:10.1021/acs.orglett.0c01264