1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

Base Information

Chemical Name:1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate
CAS No.:1418011-73-0
Molecular Formula:C₄₂H₃₂F₃NO₁₀
Molecular Weight:767.712
Hs Code.:

Synonyms:1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

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Chemical Property of 1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

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Technology Process of 1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

There total 2 articles about 1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 7143-89-7
1,3,4,5-tetra-O-benzoyl-β-D-fructopyranoside

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1418011-73-0
1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2012.11.058

Reference yield:

: 6347-01-9
fructopyranose

: 98-88-4
benzoyl chloride

: 1418011-73-0
1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / -10 °C

2: potassium carbonate / acetone / 1 h / 20 °C

With pyridine; potassium carbonate; In dichloromethane; acetone;

Reference yield: 98.0%

: 1418011-73-0
1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate

: 134136-50-8
3,4,5-tri-O-benzoyl-β-D-fructopyranoside

: C₆₁H₅₀O₁₈

Guidance literature:: 1,3,4,5-tetra-O-benzoyl-β-D-fructopyranosyl-2-(N-phenyl)trifluoroacetimidate; 3,4,5-tri-O-benzoyl-β-D-fructopyranoside; In dichloromethane; at -18 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -18 ℃; for 1.5h;