3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

Base Information

Chemical Name:3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid
CAS No.:113347-77-6
Molecular Formula:C₁₉H₁₇N₃O
Molecular Weight:303.363
Hs Code.:

Synonyms:3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

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Chemical Property of 3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

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Technology Process of 3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

There total 4 articles about 3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 113377-61-0
(E)-α-(1,2,3,4-Tetrahydro-β-carbolin-2-yl)-acetophenonoxim

: 113347-77-6
3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

Guidance literature:: With edetate disodium; mercury(II) oxide; In ethanol; at 80 - 90 ℃; for 1h;
DOI:10.1007/BF00809930

Reference yield:

: 16502-01-5
tetrahydrobetacarboline

: 113347-77-6
3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / tetrahydrofuran / 1 h

2: 2 g / NH₂OH*HCl / ethanol / 3 h / Heating

3: 50 percent / HgO/Na₂EDTA*2H₂O / ethanol / 1 h / 80 - 90 °C

With hydroxylamine hydrochloride; edetate disodium; mercury(II) oxide; In tetrahydrofuran; ethanol;
DOI:10.1007/BF00809930

Reference yield:

: 111733-93-8
α-(1,2,3,4-Tetrahydro-β-carbolin-2-yl)-acetophenon

: 113347-77-6
3,5,6,11b-Tetrahydro-2-phenyl-11H-imidazo<1',2':1,2>pyrido<3,4-b>indol-1-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: 2 g / NH₂OH*HCl / ethanol / 3 h / Heating

2: 50 percent / HgO/Na₂EDTA*2H₂O / ethanol / 1 h / 80 - 90 °C

With hydroxylamine hydrochloride; edetate disodium; mercury(II) oxide; In ethanol;
DOI:10.1007/BF00809930