methyl 5-oxo-7-phenylthioheptanoate

Base Information

• Chemical Name: methyl 5-oxo-7-phenylthioheptanoate
• CAS No.: 1031391-01-1
• Molecular Formula: C₁₄H₁₈O₃S
• Molecular Weight: 266.361
• Mol file: 1031391-01-1.mol

Synonyms:methyl 5-oxo-7-phenylthioheptanoate

Chemical Property of methyl 5-oxo-7-phenylthioheptanoate

Chemical Property:

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Technology Process of methyl 5-oxo-7-phenylthioheptanoate

There total 1 articles about methyl 5-oxo-7-phenylthioheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1-morpholin-4-yl-3-phenylsulfanyl-propan-1-one + dichloromethane (75-09-2) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → methyl 5-oxo-7-phenylthioheptanoate (1031391-01-1)

Guidance literature:

1-morpholin-4-yl-3-phenylsulfanyl-propan-1-one; dichloromethane; With titanium tetrachloride; magnesium; In tetrahydrofuran; at 0 ℃; for 1h;

acrylic acid methyl ester; With triethylamine; In tetrahydrofuran; dichloromethane; at 0 - 25 ℃; for 2h; Further stages.;

DOI:10.1021/jo800732s

upstream raw materials:

dichloromethane

acrylic acid methyl ester