4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

Base Information

Chemical Name:4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone
CAS No.:701285-10-1
Molecular Formula:C₄₁H₃₄N₄O₁₁S
Molecular Weight:790.807
Hs Code.:

Synonyms:4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

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Chemical Property of 4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

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Technology Process of 4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

There total 3 articles about 4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 701285-03-2
4-benzyloxy-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 701285-10-1
4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h;
DOI:10.1081/NCN-120027817

Reference yield:

: 701285-00-9
6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 701285-10-1
4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver carbonate / benzene / 2 h / 80 °C

1.2: 14 percent / benzene / 48 h / 60 - 70 °C

2.1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 12 h

With 3-chloro-benzenecarboperoxoic acid; silver carbonate; In dichloromethane; benzene;
DOI:10.1081/NCN-120027817

Reference yield:

: 138612-37-0
6-methyl-2-methylthio-4(3H),7(8H)-pteridinedione

: 701285-10-1
4-benzyloxy-6-methyl-2-methylsulfonyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7(8H)-pteridinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: (NH₄)2SO₄; hexamethyldisilazane / 6 h / Heating

1.2: 45 percent / BF₃-etherate / CH₂Cl₂ / 24 h / 20 °C

2.1: silver carbonate / benzene / 2 h / 80 °C

2.2: 14 percent / benzene / 48 h / 60 - 70 °C

3.1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 12 h

With ammonium sulfate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; silver carbonate; In dichloromethane; benzene;
DOI:10.1081/NCN-120027817