N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

Base Information

Chemical Name:N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine
CAS No.:53097-55-5
Molecular Formula:C₁₃H₂₅NSi
Molecular Weight:223.434
Hs Code.:

Synonyms:N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

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Technology Process of N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

There total 1 articles about N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 766-05-2
cyclohexane carbonitrile

: 18162-48-6
tert-butyldimethylsilyl chloride

: 53097-55-5
N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

Guidance literature:: cyclohexane carbonitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

tert-butyldimethylsilyl chloride; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201406181

Reference yield: 93.0%

: 53097-55-5
N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

: 1373942-84-7
tert-butyl (1-benzyl-2-oxoindolin-3-ylidene)carbamate

: tert-butyl (1-benzyl-3-(1-cyanocyclohexyl)-2-oxoindolin-3-yl)carbamate

Guidance literature:: With C₃₁H₄₀N₄O₄; zinc trifluoromethanesulfonate; In tetrahydrofuran; at -45 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201408730

Reference yield: 92.0%

: 100-54-9,121697-66-3,1232169-17-3,68271-95-4
pyridine-3-carbonitrile

: 53097-55-5
N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine

: 4-(1-cyanocyclohexyl)nicotinonitrile

Guidance literature:: pyridine-3-carbonitrile; N-(cyclohexaneylidenemethylene)-1-(1,1-dimethylethyl)-1,1-dimethylsilanamine; With C₂₆H₁₇F₆N₂O₆PS₂; In acetonitrile; at 20 ℃; for 20h; Inert atmosphere; Sealed tube;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1021/jacs.1c03257