5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

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Chemical Name:5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine
CAS No.:1542260-33-2
Molecular Formula:C₅H₅N*C₄₀H₄₈N₂O₁₁Si
Molecular Weight:844.975
Hs Code.:

Synonyms:5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

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Chemical Property of 5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

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Technology Process of 5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

There total 5 articles about 5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-30-5
succinic acid anhydride

: 1542260-23-0
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 1542260-33-2
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Guidance literature:: With pyridine; dmap; at 37 ℃; for 14h;

Reference yield:

: 110-86-1
pyridine

: 108-30-5
succinic acid anhydride

: 1542260-23-0
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 1542260-33-2
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Guidance literature:: With dmap; at 37 ℃; for 14h; Sealed tube;

Reference yield:

: 2′,3′,5′-trihydroxy-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

: 1542260-33-2
5′-O-dimethoxytrityl-2′-O-tert-butyldimethylsilyl-3'-O-succinyl pyridinium salt-2′,3′,4′,5′,5″-pentadeuterium-β-D-ribofuranosyl uridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 5 h / 0 °C

2.1: silver nitrate; pyridine / tetrahydrofuran / 0.17 h / 20 °C

2.2: 2.5 h / 20 °C / Sealed tube

3.1: dmap / 14 h / 37 °C / Sealed tube

With pyridine; dmap; silver nitrate; In tetrahydrofuran;