3-(4-cyano-benzoylamino)-2-chloropyridine

Base Information

• Chemical Name: 3-(4-cyano-benzoylamino)-2-chloropyridine
• CAS No.: 126921-78-6
• Molecular Formula: C₁₃H₈ClN₃O
• Molecular Weight: 257.679
• Mol file: 126921-78-6.mol

Synonyms:3-(4-cyano-benzoylamino)-2-chloropyridine

Chemical Property of 3-(4-cyano-benzoylamino)-2-chloropyridine

Chemical Property:

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Technology Process of 3-(4-cyano-benzoylamino)-2-chloropyridine

There total 1 articles about 3-(4-cyano-benzoylamino)-2-chloropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-chloro-3-aminopyridine (6298-19-7) + 4-cyanobenzoyl chlorIde (6068-72-0) → 3-(4-cyano-benzoylamino)-2-chloropyridine (126921-78-6)

Guidance literature:

In pyridine; 1. -10 deg C 2. 15h, r. t.;

Reference yield: 98.0%

3-(4-cyano-benzoylamino)-2-chloropyridine (126921-78-6) → 2-(4-cyano-phenyl)oxazolo<5,4-b>pyridine (52334-01-7)

Guidance literature:

With trimethylsilylpolyphosphate ester; In various solvent(s); for 15h; Heating;

upstream raw materials:

2-chloro-3-aminopyridine

4-cyanobenzoyl chlorIde

Downstream raw materials:

2-(4-cyano-phenyl)oxazolo<5,4-b>pyridine

Refernces