(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Base Information

Chemical Name:(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)
CAS No.:1334246-13-7
Molecular Formula:C₂₂H₁₉F₃N₂O₂S
Molecular Weight:432.466
Hs Code.:

Synonyms:(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Suppliers and Price of (N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Chemical Property:

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Technology Process of (N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

There total 6 articles about (N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.7%

: 1334246-07-9
(N-(5,8-Dimethyl-9H-carbazol-1-yl)-3-trifluoromethylbenzenesulfonamide)

: 74-88-4
methyl iodide

: 1334246-13-7
(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Guidance literature:: (N-(5,8-Dimethyl-9H-carbazol-1-yl)-3-trifluoromethylbenzenesulfonamide); With potassium hydroxide; In ethanol; at 70 ℃; for 0.25h;

methyl iodide; In ethanol; at 70 ℃; for 1h;

Reference yield:

: 6960-45-8
7-nitro-1H-indole-2-carboxylic acid

: 1334246-13-7
(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(II) oxide / quinoline / 2 h / 194 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h

3.1: ethyl acetate / 1 h / 50 °C

3.2: 3 h / Reflux

4.1: potassium hydroxide / ethanol / 0.25 h / 70 °C

4.2: 1 h / 70 °C

With hydrogen; potassium hydroxide; palladium 10% on activated carbon; copper(II) oxide; In quinoline; methanol; ethanol; ethyl acetate;

Reference yield:

: 6960-46-9
ethyl 7-nitroindole-2-carboxylate

: 1334246-13-7
(N-(5,8-Dimethyl-9H-carbazol-1-yl)-N-methyl-3-trifluoromethylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; water / ethanol / 40 °C

2.1: copper(II) oxide / quinoline / 2 h / 194 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h

4.1: ethyl acetate / 1 h / 50 °C

4.2: 3 h / Reflux

5.1: potassium hydroxide / ethanol / 0.25 h / 70 °C

5.2: 1 h / 70 °C

With water; hydrogen; potassium hydroxide; palladium 10% on activated carbon; copper(II) oxide; In quinoline; methanol; ethanol; ethyl acetate;