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{Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN

Base Information Edit
  • Chemical Name:{Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN
  • CAS No.:109862-72-8
  • Molecular Formula:C52H42Mn3N2O14
  • Molecular Weight:1104.25
  • Hs Code.:
  • Mol file:109862-72-8.mol
{Mn<sub>3</sub>O(O<sub>2</sub>CPh)6(pyridine)2(H<sub>2</sub>O)}*0.5CH<sub>3</sub>CN

Synonyms:{Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN

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Chemical Property of {Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN Edit
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Technology Process of {Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN

There total 1 articles about {Mn3O(O2CPh)6(pyridine)2(H2O)}*0.5CH3CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With pyridine; In ethanol; acetic acid; aerobic conditions, Mn compd., acid dissolved in solvent mixture, solid ammonium salt added under stirring,; after 24 h ppt. filtered off, ppt. washed with EtOH, dried in vac., crude yield:>95%; recrystn. by allowing an acetonitrile soln. to slowly concentrate by evapn., ppt. filtered off, washed with EtOH, dried in vac., elem. anal.;
DOI:10.1021/ja00253a023
Guidance literature:
In acetonitrile; Mn-complex and ligand dissolved in MeCN, stirred for 10 min, transferredinto glass tube, heated with microwave at 120°C for 5 min, coole d; filtered, allowed to stand for 48 h, collected, washed with MeCN, dried in air; elem. anal.;
DOI:10.1039/b901121h
Guidance literature:
With NEt3; In ethanol; acetonitrile; byproducts: PhCO2H; NEt3 added in small portions to stirred soln. of Mn complex in MeCN-EtOH; stirred for 20 min; filtered; filtrate layered with Et2O; left undisturbed at ambient temp. for 2 d; filtered; crystals washed with Et2O; dried in vac.; elem. anal.;
DOI:10.1021/ic801484g
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