4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

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Chemical Name:4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone
CAS No.:332077-61-9
Molecular Formula:C₂₉H₃₂O₇
Molecular Weight:492.569
Hs Code.:

Synonyms:4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

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Chemical Property of 4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

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Technology Process of 4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

There total 5 articles about 4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 332077-60-8
1-(p-benzyloxy-m-methoxyphenyl)-1-(2,3-dimethoxy)-5-(5',5'-dimethyl-1',3'-dioxan-2'-yl)phenyl carbinol

: 332077-61-9
4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4039(00)02163-8

Reference yield:

: 2973-76-4
5-bromo-4-hydroxy-3-methoxybenzaldehyde

: 332077-61-9
4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammonium iodide; NaOH / CH₂Cl₂; H₂O / 20 °C

2.1: 58 percent / p-TsOH / Heating

3.1: nBuLi / -78 °C

3.2: 77 percent / -78 °C

4.1: 96 percent / MnO₂ / CH₂Cl₂ / 20 °C

With manganese(IV) oxide; sodium hydroxide; n-butyllithium; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)02163-8

Reference yield:

: 6948-30-7
5-bromoveratralaldehyde

: 332077-61-9
4-benzyloxy-3-methoxyphenyl 5-(5,5-dimethyl-1,3-dioxan-2-yl)-2,3-dimethoxyphenyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 58 percent / p-TsOH / Heating

2.1: nBuLi / -78 °C

2.2: 77 percent / -78 °C

3.1: 96 percent / MnO₂ / CH₂Cl₂ / 20 °C

With manganese(IV) oxide; n-butyllithium; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)02163-8