distigmine bromide

Base Information

• Chemical Name: distigmine bromide
• CAS No.: 15876-67-2
• Molecular Formula: C22H32Br2N4O4
• Molecular Weight: 576.328
• Mol file: 15876-67-2.mol

Synonyms:3-Hydroxy-1-methylpyridiniumbromide, hexamethylenebis[methylcarbamate] (6CI,7CI);Pyridinium,3,3'-[1,6-hexanediylbis[(methylimino)carbonyl]oxy]bis[1-methyl-, dibromide(9CI);Pyridinium, 3-hydroxy-1-methyl-, bromide,hexamethylenebis[methylcarbamate] (2:1) (8CI);BC 51;Distigmine bromide;Distigmine dibromide;Hexamarium;N,N'-Hexamethylenebis(3-N-methylcarbamoxy-1-methylpyridine)dibromide;Ubretid;Ubritil;3,3'-{1,6-Hexanediylbis[(methylcarbamoyl)oxy]}bis(1-methylpyridinium) dibromide;

Chemical Property of distigmine bromide

Chemical Property:

• PSA: 66.84000
• LogP: -3.53460
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

DistigmineBromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of distigmine bromide

There total 2 articles about distigmine bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl bromide (74-83-9) + Methyl-{6-[methyl-(pyridin-3-yloxycarbonyl)-amino]-hexyl}-carbamic acid pyridin-3-yl ester (95701-58-9) → BC 51 (15876-67-2)

Guidance literature:

In acetone; at 0 ℃;

Reference yield:

N,N'-dimethyl-N,N'-hexanediyl-bis-carbamoyl chloride (99191-71-6) → BC 51 (15876-67-2)

Guidance literature:

With xylene; at 80 ℃; Behandeln einer Loesung des Reaktionsprodukts in Aceton mit Methylbromid;

upstream raw materials:

N,N'-dimethyl-N,N'-hexanediyl-bis-carbamoyl chloride

methyl bromide

Methyl-{6-[methyl-(pyridin-3-yloxycarbonyl)-amino]-hexyl}-carbamic acid pyridin-3-yl ester